Completed funded project

Development of a coating of short fibres using the fluidised bed coating process (FRG-3D)

Motivation

Process flow for the production of SiC short fibres as well as for the subsequent coating of the fibres
© Fraunhofer-Center HTL
Process flow for the production of SiC short fibres as well as for the subsequent coating of the fibres

The overall objective of the project is the additive production of fibre-reinforced SiC/SiC and C/SiC components with significant property and environmental advantages over conventionally processed ceramics. The first step is the development of fibre-filled granulates for the additive production of short fibre reinforced preforms, which are further processed by reactive infiltration with molten silicon to form complex Ceramic Matrix Composites (CMC) structures. Short fibre or particle-reinforced CMC with isotropic properties are particularly suitable for the manufacture of geometrically complex but compact components which are subjected to high loads in different load combinations and load directions and additionally to very high temperatures. Examples are fittings of all kinds as well as nozzles, combustion chambers, turbine parts, brake discs, high-temperature fans or structural parts for optics.

Objective

Cladding surface of a SiC short fibre with 2-fold boron nitride coating: The diagram shows an EDX analysis of the cladding surface to verify the boron nitride coating
© Fraunhofer-Center HTL
Cladding surface of a SiC short fibre with 2-fold boron nitride coating: The diagram shows an EDX analysis of the cladding surface to verify the boron nitride coating

Within the scope of the individual project of the Fraunhofer-Center HTL, a coating of ceramic short fibres using a fluidised coating process is to be developed. Ideally, the short fibres should be completely covered with a boron nitride coating so that the end faces are also coated. The coating is intended to adjust the bonding of the fibres to the matrix in such a way that an improvement of the mechanical characteristics of the additive produced short fibre reinforced CMC is achieved. The coated short fibres are processed by the project partners into CMC by means of additive manufacturing processes.

Results

Demonstrator component: 3D printed gas guide tube
© Foto: ArianeGroup GmbH
Demonstrator component: 3D printed gas guide tube
  • Milling process for the production of SiC short fibres with defined average lengths successfully developed
  • Scalable, cost-effective dip coating process successfully developed
  • Complete cladding of SiC short fibres with boron nitride coating
  • Boron nitride coatings are crystalline with desired hexagonal modification
  • Boron nitride coatings without oxygen impurities
    → improved thermal stability of the coatings

Project Data

Project Duration 01.04.2019 - 31.12.2022
Sponsor Bavarian State Ministry of Economic Affairs, Regional Development and Energy
Funding Amount 50.000 Euro
Project Partners Fraunhofer-Center HTL
Ariane Group GmbH
Kyocera FineCeramics GmbH
Project Coordination Ariane Group GmbH
Project Management at the HTL Dr. Andreas Nöth